Views: 0 Author: Site Editor Publish Time: 2025-06-05 Origin: Site
Engine coolants (antifreeze mixtures) incorporate additives—corrosion inhibitors, pH buffers, and anti-foaming agents—that leave behind inorganic residues when the fluid is subjected to high temperatures or combustion byproducts. The Engine Coolant Ash Content Tester from Changsha Friend Experimental Analysis Instrument Co., Ltd. measures these nonvolatile residues, commonly referred to as “ash,” ensuring that coolant quality remains within specification and reducing the risk of deposit formation in radiators and engine passages.
Deposits of metallic or inorganic ash can restrict coolant flow, insulate heat-transfer surfaces, and lead to localized hot spots. Over time, this can cause head gasket failure, blockages, and reduced engine efficiency. By quantifying ash content, laboratories can:
Verify the depletion rate of inhibitor packages.
Identify contamination from engine blow-by or external particulates.
Predict maintenance intervals to prevent scale build-up.
Confirm that refill or bulk coolant meets OEM performance requirements.
The instrument is based on a gravimetric ashing method:
Sample Preparation: A defined volume (e.g., 50 mL) of coolant is evaporated to dryness in a porcelain or quartz crucible.
Ignition: The dried residue is incinerated in a programmable muffle furnace at a controlled temperature (commonly 500–550 °C) for a specified dwell time (often 2 hours) to volatilize organic components.
Cooling and Weighing: After ashing, the crucible is cooled in a desiccator and weighed on a high-precision balance (±0.1 mg).
Calculation: The percentage of ash is calculated relative to the initial sample mass.
Programmable Muffle Furnace: Ramp rates and hold times are user-selectable, ensuring consistent combustion of organics without sintering inorganic residues.
High-Accuracy Analytical Balance: Typically integrated or paired with the furnace workflow to minimize handling errors.
Temperature Uniformity: Insulated furnace chamber with ±2 °C uniformity at ashing temperatures.
Crucible Rack and Handling Tools: Ensures safe transfer from furnace to balance without thermal shock or contamination.
Intuitive Software Interface: Allows users to program test methods, track test batches, and generate certificates of analysis.
Coolant Manufacturers: R&D teams monitor ash formation during accelerated aging studies to optimize additive chemistry.
Automotive OEM Labs: Validate that coolant formulations meet GM GM6041M, Ford WSS-M97B51-A1, or similar specifications for maximum inorganic residue.
Service Centers: Large-volume coolant exchange facilities check batch quality before distribution to repair shops.
Heavy-Duty Engines: Diesel engine manufacturers, where high combustion byproducts can increase ash in cooling systems, use ash testing to determine coolant change intervals.
Sample Collection: Collect coolant in clean, airtight containers to prevent dust or suspended particles from skewing results.
Crucible Conditioning: Pre-bake crucibles at ashing temperature to remove any residual moisture or contaminants before use.
Furnace Calibration: Use certified thermocouples to verify actual chamber temperature versus setpoint; adjust offsets as needed.
Weighing Protocol: Allow crucibles to cool to room temperature in a desiccator for at least 20 minutes before weighing to avoid buoyancy errors.
Replicate Testing: Run samples in duplicate to confirm repeatability; discard outliers and calculate average ash content.
By employing the Engine Coolant Ash Content Tester, laboratories can proactively manage deposit risk, confirm additive package integrity, and support optimal engine cooling system performance.
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